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Spray silvering proportions & recipe

Base quantity is 150ml distilled water + 1.6g silver nitrate.
Other quantities are derived from that.
Recipe from Gerhard S. on Cloudy Nights

BOM for a session

Gloves
Chalk to wash the mirrors
Mirror stands
Anti-projection box
Hairdryer
Hydrophilic cotton
Demin. water
Stands for the mirrors
A box in which to silver
Glucose
Silver nitrate
Sodium hydroxide
Ammonia
Two sprayers
Containers
FFP2 masks

The chemicals

Step 0

Calibrate bottles

Calibrate Bottle 1 and Bottle 2 with water, ensuring that the same quantity of water is sprayed with 100 sprays.

Step 1

Prepare the solutions

Solution 1: 1.6g silver nitrate + 150ml distilled water

Solution 2: 2.5g sodium hydroxide + 150ml distilled water

Solution 3: 12g glucose + 300ml distilled water

Bottle 1 is the mixed solution according to below instructions.

Bottle 2 contains the sugar Solution 3

Step 2

Mixing of silver solution

(becomes Bottle 1)

  • 1 : Pour about 100ml ml of Solution 1 into a mixing bowl.
  • 2 : Add a few drops of ammonia solution (25% dilution)
  • 3 : Add all of Solution 2
  • 4 : Add the rest of Solution 1 (the solution will turn brown)
  • 5 : Carefully add ammonia solution drop by drop while stirring until a transparent, slightly brownish solution is obtained.

Any precipitate that may still be present should be completely dissolved


The cleaning and spraying

Clean the mirror

Use chalk precipitate in distilled/demin water on small cotton balls. Change often and start with thick sauce, thinning it progressively. The center will clean fast but the edge and chamfer need a LOT of time.

Rough guideline : (diameter_in_mm/15)^1.4 = time.
Yes, that is an advice of 1h40 for a 400mm mirror.

Rinse with demin water and if possible, high pressure.

Create optical pieces in the Hardware tab to quickly load their dimensions here.

Cleaning time : 0h25m


Spray the mirror

Spray the mirror with both sprays, ensuring that they mix on the surface. You will see a faint blue film appear first.
Then it will turn yellowish. If you see dark brown or black streaks, this means your cleaning wasn't thorough enough.
A thin coating is preferable to a thick one and it should still be a tad transparent at the end.

Dry & store

Immediately dry with a hot air gun and store in an airtight box with dessicant packs, or better, silver protector felt. Silver protector felt is felt impregnated with tiny silver particles that are there to react with oxydants first and protect your coating.

A project by Lucas Sifoni, Paul Faÿs from Gallifrey Optics, and Raphaël Labro from La3emedim.fr
Contribute on github.

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